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Analytical Methods for Coal and Coal Products. Volume II - download pdf or read online

By Clarence Karr (Eds.)

ISBN-10: 0123999022

ISBN-13: 9780123999023

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Extra info for Analytical Methods for Coal and Coal Products. Volume II

Sample text

B l o m and co-workers hydrolyzed the acetylated product and titrated the a c e t i c a c i d r e l e a s e d . Hill a n d G i v e n (1969) r e p l a c e d t h i s t e d i o u s p r o c e 1 4 dure b y using C - l a b e l e d acetic anhydride and determining the acetyl u p t a k e r a d i o c h e m i c a l l y . A b d e l - B a s e t et al. (1978) h a v e m o d i f i e d t h i s p r o c e d u r e further b y c o m b u s t i n g t h e p r o d u c t a n d a b s o r b i n g t h e g a s for liquid scintillation counting.

As a s e p a r a t e crystal p h a s e , t h i s m i n e r a l is s o l u b l e i n a c i d , y i e l d i n g H 2 S , so that its determination w o u l d appear simple. H o w e v e r , a research w o r k e r s t u d y i n g k i n e t i c s a n d m e c h a n i s m s m i g h t w e l l h a v e a n e e d to determine pyrrhotite in a solid product formed w h e n the level of conv e r s i o n h a s d e l i b e r a t e l y b e e n h e l d l o w , so that p y r i t e m a y h a v e b e e n i n c o m p l e t e l y r e d u c e d .

V o l b o r t h et al. (1977a) c o n c e d e t h a t it w o u l d b e useful to h a v e t h e o x y g e n c o n t e n t s o f the low temperature ash of samples studied, b u t evidently did not have a c c e s s to t h e t e c h n i q u e . A c c o r d i n g l y , t h e y e q u a t e d t h e m e a n o x y g e n content of the h i g h temperature ashes of eight coals w i t h the inorganic o x y g e n c o n t e n t s o f e a c h coal. T h i s is totally i n a d m i s s i b l e . H a m r i n et al.

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Analytical Methods for Coal and Coal Products. Volume II by Clarence Karr (Eds.)


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